Title Information
Title
Development of an Analytical Method for Polymeric Nanoparticle Quantification in Serum by Fourier Transform-Infrared Spectroscopy
Type of Resource
text
Name: Personal
Name Part
Nguyen, Travis
Role
Role Term: Text
creator
Name: Personal
Name Part
Mathiowitz, Edith
Role
Role Term: Text
Advisor
Name: Personal
Name Part
Srivastava, Vikas
Role
Role Term: Text
Reader
Name: Personal
Name Part
Furtado, Stacia
Role
Role Term: Text
Reader
Name: Corporate
Name Part
Brown University. Department of Molecular Pharmacology, Physiology and Biotechnology
Role
Role Term: Text
sponsor
Origin Information
Copyright Date
2019
Physical Description
Extent
vi, 35 p.
digitalOrigin
born digital
Note: thesis
Thesis (Sc. M.)--Brown University, 2019
Genre (aat)
theses
Abstract
This work aims to develop a method of using Fourier-Transform Infrared Spectroscopy (FT-IR) for quantification of polymer levels in biological samples, ex vivo. A method of producing a calibration curve for Sprague Dawley rat serum and PLA nanoparticles (NP) was developed, and tested for reproducibility and feasibility. Individual samples were prepared from stock solutions of potassium bromide (KBr), the biological sample (rat serum), and Poly-L-Lactic Acid (8 kDa) nanoparticles. For each interferogram at a given concentration of PLA, ratios between the absorbance peaks near 1650 and 1750 〖cm〗^(-1 )were recorded. Linearity was shown within 2.5-10% of PLA: serum (w/w) and this relationship was used to calculate NP absorption in vivo. The results show promise in the method’s ability to detect and quantify biodegradable polymers in serum.
Subject (fast) (authorityURI="http://id.worldcat.org/fast", valueURI="http://id.worldcat.org/fast/00898667")
Topic
Drug delivery systems
Subject
Topic
Polymeric nanoparticles
Subject
Topic
FT-IR
Subject
Topic
Quantification
Language
Language Term (ISO639-2B)
English
Record Information
Record Content Source (marcorg)
RPB
Record Creation Date (encoding="iso8601")
20190603
Identifier: DOI
10.26300/7gmx-w627
Access Condition: rights statement (href="http://rightsstatements.org/vocab/InC/1.0/")
In Copyright
Access Condition: restriction on access
All rights reserved. Collection is open to the Brown community for research.